From: Architectures of archaeal GINS complexes, essential DNA replication initiation factors
Data Collection Summary | Â | Â | Â | Â | Â |
---|---|---|---|---|---|
 |  |  | Derivative |  |  |
 |  | Native | Ta6Br14 | SeMet | K2PtCl4 |
Wavelength | (Ã…) | 1.0000 | 1.2544 | 0.9795 | 1.0717 |
Resolution | (Ã…) | 50.0-2.65 | 50.0-3.16 | 50.0-2.80 | 50.0-3.19 |
(Highest shell) | Â | (2.74-2.65) | (3.27-3.16) | (2.90-2.80) | (3.30-3.19) |
Measured reflections | Â | 227882 | 127012 | 181671 | 112023 |
Unique reflections | Â | 16278 (1598) | 9676 (901) | 13780(1256) | 9034 (921) |
Completeness | (%) | 99.4 (100.0) | 97.6 (95.1) | 99.1 (92.8) | 94.5 (99.9) |
I/σ(I) |  | 17.6 (9.9) | 23.8 (11.4) | 14.5 (7.1) | 14.2 (7.4) |
Redundancy | Â | 14.0 (14.0) | 13.1 (13.5) | 13.2 (9.7) | 12.4 (9.3) |
R merge | (%) | 4.3 (38.8) | 5.6 (23.0) | 7.5 (33.9) | 6.7 (38.6) |
MIRAS Phasing Statistics | Â | Â | Â | Â | Â |
Riso(F) (%) | Â | Â | 12.4 | 21.1 | 17.1 |
Number of Sites | Â | Â | 2 | 6 | 1 |
Resolution | (Ã…) | Â | 50.0-4.0 | 50.0-4.0 | 50.0-4.0 |
Phasing Power (Centric/Acentric) | Â | Â | 0.56/0.57 | 0.64/0.54 | 0.63/0.62 |
Figure of merit (Centric/Acen.) | Â | 0.32/0.36 | Â | Â | Â |
Refinement | Â | Â | Â | Â | Â |
Resolution | (Ã…) | 50.0-2.65 | Â | Â | Â |
Rwork/Rfreea | (%) | 25.7/29.7 | Â | Â | Â |
Number of atoms | Â | Â | Â | Â | Â |
Protein | Â | 2623 | Â | Â | Â |
Water | Â | 33 | Â | Â | Â |
Average B-factor | (Ã…2) | Â | Â | Â | Â |
Protein | Â | 65.7 | Â | Â | Â |
Water | Â | 56.9 | Â | Â | Â |
r.m.s.d. | Â | Â | Â | Â | Â |
Bond Lengths | (Ã…) | 0.01 | Â | Â | Â |
Angles | (°) | 1.364 |  |  |  |
PDB code | Â | 3ANW | Â | Â | Â |