Crystal data | Â |
 Beam-line | 19-ID APS |
 Wavelength, Å | 0.97915 |
 Space group | P 21 |
 Cell constants | a = 75.6 Å, b = 106.6 Å, c = 92.1 Å, β = 105.8° |
 Resolution, Å | 2.60 |
 Total reflections | 214,320 |
 Unique reflections | 43,019 |
 Completeness, % | 99.0 (97.3) |
 I/σ | 8.9 (1.8) |
 Rsym, % | 12.9 (47.2) |
Refinement statistics | Â |
 Reflection range used, Å | 2.60–44.32 |
 No. reflections used | 42,950 |
 Rwork/Rfree, % | 18.8/23.3 |
 rmsd bonds, Å | 0.0046 |
 rmsd angle, ° | 0.791 |
 Ramachandran plot (preferred/allowed), % | 96.6/3.4 |
No. of atoms | Â |
 Protein | 10,901 |
 Metal ions | 4 |
 Waters | 263 |